反应详情

A mixture of 350 g of DMAPMA and 280 g of chlorododecene (1.5:1) was stirred with 111.2 g of water (15%) and 6 drops of concentrated sulfuric acid. The reaction mixture was heated up to 95°0 C. and N2 was bubbled through it. The conversion was followed by GC. After 24 hours the reaction mixture was cooled off (95% conversion of vinyl chloride) and product was further used in polymerization without purification.

1. temperatureThe reaction mixture was heated up to 95°0 C
2. customand N2 was bubbled through it
3. temperatureAfter 24 hours the reaction mixture was cooled off (95% conversion of vinyl chloride) and product
4. customwas further used in polymerization without purification