Isopropanol → 2,3,3,4,4-Pentafluorocyclobutenyl isopropyl ether
반응식
[OH-].[K+].F[C:4]1[C:7]([F:9])([F:8])[C:6]([F:11])([F:10])[C:5]=1[F:12].[CH:13]([OH:16])([CH3:15])[CH3:14]>C(OCC)C>[CH:13]([O:16][C:4]1[C:7]([F:8])([F:9])[C:6]([F:10])([F:11])[C:5]=1[F:12])([CH3:15])[CH3:14]참가 물질
5
실험 절차
70 g (1.23 mol) of powdered potassium hydroxide are metered into a solution of 200 g (1.23 mol) of 1,2,3,3,4,4-hexafluorocyclobutene and 90 g (1:5 mol) of isopropanol in 800 ml of diethyl ether at room temperature. The mixture is stirred for a further hour and worked up as described in Example 1. The product is then distilled.
후처리
- distillationThe product is then distilled
출처 및 근거
- ORD 기록
- ord-bfef5c94b8544c07810aa926c21820e5
- 출처 데이터셋
- uspto-grants-1992_02
- 특허 번호
- US05087775
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