Hydrochloric Acid → HCID 19908400, 화합물

HRID 1534844노트

반응식

HRID 1534844 반응식
[O-:1][C:2]#[N:3].[K+].[C:5]([NH:10][NH2:11])([CH2:8][CH3:9])([CH3:7])[CH3:6].Cl>O>[C:5]([NH:10][NH:11][C:2]([NH2:3])=[O:1])([CH2:8][CH3:9])([CH3:7])[CH3:6]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 117546HCID 117546, 화합물HCID 11378442Potassium cyanate

생성물 1

HCID 19908400HCID 19908400, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

13.6 g of potassium cyanate are added to a mixture of 17 g of tert-pentylhydrazine and 30 ml of water cooled in an ice bath and 16.5 g of conc. hydrochloric acid are then added dropwise. The mixture is stirred at room temperature for 3 h and the solid is filtered off with suction, washed with water and dried in vacuo.

후처리

  1. temperaturecooled in an ice bath
  2. filtrationthe solid is filtered off with suction
  3. washwashed with water
  4. customdried in vacuo

출처 및 근거

ORD 기록
ord-4d8ee08daba343dfb7c4cd34613a8364
출처 데이터셋
uspto-grants-1992_02
특허 번호
US05091398

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