Chlorine → HCID 57368802, 화합물
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[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[Cl:11])[CH:5]=[N:6][OH:7].[Cl:12]Cl>C(Cl)(Cl)Cl>[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][C:10]=1[Cl:11])[C:5]([Cl:12])=[N:6][OH:7]참가 물질
4
실험 절차
A cold solution of 18.9 g of 3,4-dichlorobenzaldoxime in 150 ml of chloroform was treated with chlorine gas until no more chlorine was absorbed. The green mixture was stirred for 1 hour at 5°, then heated under reflux for 30 minutes, when the solid went into solution and the clear green solution changed to yellow. The solution was evaporated under reduced pressure to give a white solid, m.p. 104°-106°, which was used without further purification.
후처리
- customwas absorbed
- temperatureheated
- temperatureunder reflux for 30 minutes
- customThe solution was evaporated under reduced pressure
- customto give a white solid, m.p. 104°-106°, which
- customwas used without further purification
출처 및 근거
- ORD 기록
- ord-3e43abe111424d88ba0b5ca08bc2e768
- 출처 데이터셋
- uspto-grants-1976_09
- 특허 번호
- US03983246
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