p-Anisoyl chloride → HCID 86734036, 화합물
반응식
C(C1OC2C=CC(Br)=CC=2C=1)C1C=CC=CC=1.C(Cl)(=O)C1C=CC(OC)=CC=1.[CH2:29]([C:36]1[O:37][C:38]2[CH:54]=[CH:53][C:52]([Br:55])=[CH:51][C:39]=2[C:40]=1[C:41](=[O:50])[C:42]1[CH:47]=[CH:46][C:45]([O:48][CH3:49])=[CH:44][CH:43]=1)[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1.[C:56]([N:60]1[CH2:63][CH:62](CCl)[CH2:61]1)([CH3:59])([CH3:58])[CH3:57]>>[CH2:29]([C:36]1[O:37][C:38]2[CH:54]=[CH:53][C:52]([Br:55])=[CH:51][C:39]=2[C:40]=1[C:41](=[O:50])[C:42]1[CH:47]=[CH:46][C:45]([O:48][CH2:49][C:61]2[C-:62]=[CH:63][N+:60]=2[C:56]([CH3:59])([CH3:58])[CH3:57])=[CH:44][CH:43]=1)[C:30]1[CH:31]=[CH:32][CH:33]=[CH:34][CH:35]=1참가 물질
5
실험 절차
2-Benzyl-5-bromobenzofuran is acylated with p-anisoyl chloride as described above, the resulting 2-benzyl-5-bromo-3-(4-methoxybenzoyl)benzofuran is dimethylated and the product thus formed is reacted with N-t-butyl-3-chloromethylazetidine as described in Example 3 to give the title compound.