Hydrochloric Acid → Sulfanilamide Hydrochloric Acid Brij 35

HRID 1578220노트

반응식

HRID 1578220 반응식
[S:1]([NH2:11])(=[O:10])([C:3]1[CH:8]=[CH:7][C:6]([NH2:9])=[CH:5][CH:4]=1)=[O:2].[CH3:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:24][CH2:25][CH2:26][OH:27].[ClH:28]>O>[S:1]([NH2:11])(=[O:10])([C:3]1[CH:4]=[CH:5][C:6]([NH2:9])=[CH:7][CH:8]=1)=[O:2].[ClH:28].[CH3:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][O:24][CH2:25][CH2:26][OH:27]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 5333Sulfanilamide2회HCID 247502-(Dodecyloxy)ethanol

생성물 1

HCID 131712428Sulfanilamide Hydrochloric Acid Brij 35

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

To a 2 liter volumetric flask containing approximately 1500 ml. of distilled water is added 20.0 g. of sulfanilamide (0.116 mol), 66 ml. of Brij 35 and 200 ml. of concentrated hydrochloric acid. The resulting mixture is taken up to 2 liters with distilled water and then stirred until the sulfanilamide is completely dissolved.

후처리

  1. additionTo a 2 liter volumetric flask containing approximately 1500 ml
  2. dissolutionis completely dissolved

출처 및 근거

ORD 기록
ord-5bde5d665a8e41d9bcf7e6b78f5c52a5
출처 데이터셋
uspto-grants-1981_09
특허 번호
US04292040

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