tert-Butyl mercaptan → 4-(Tert-butylthio)-7-nitro-2,5-bis-(trifluoromethyl)benzimidazole

HRID 1578737노트

반응식

HRID 1578737 반응식
Cl[C:2]1[C:10]2[NH:9][C:8]([C:11]([F:14])([F:13])[F:12])=[N:7][C:6]=2[C:5]([N+:15]([O-:17])=[O:16])=[CH:4][C:3]=1[C:18]([F:21])([F:20])[F:19].[K].[C:23]([SH:27])([CH3:26])([CH3:25])[CH3:24]>>[C:23]([S:27][C:2]1[C:10]2[NH:9][C:8]([C:11]([F:14])([F:13])[F:12])=[N:7][C:6]=2[C:5]([N+:15]([O-:17])=[O:16])=[CH:4][C:3]=1[C:18]([F:21])([F:20])[F:19])([CH3:26])([CH3:25])[CH3:24]

참가 물질

4

반응물 3

HCID 6387tert-Butyl mercaptanHCID 5462222PotassiumHCID 1355549354-Chloro-7-nitro-2,5-bis(trifluoromethyl)benzimidazole

생성물 1

HCID 215585754-(Tert-butylthio)-7-nitro-2,5-bis-(trifluoromethyl)benzimidazole

실험 절차

4-Chloro-7-nitro-2,5-bis(trifluoromethyl)benzimidazole is reacted with the potassium derivative of tertbutanethiol to obtain 4-(tert-butylthio)-7-nitro-2,5-bis-(trifluoromethyl)benzimidazole, m.w., 387.3.

출처 및 근거

ORD 기록
ord-7a053d79260e40ba8ca5d6887bbdb73b
출처 데이터셋
uspto-grants-1976_02
특허 번호
US03939166

반응 노트

불러오는 중…