Sodium Carbonate → Triallyl phosphate
반응식
C(=O)([O-])[O-:2].[Na+].[Na+].C(=O)(O)[O-].[Na+].[Cr](O[Cr]([O-])(=O)=O)([O-])(=O)=O.[K+].[K+].[P:23]([O:32][CH2:33][CH:34]=[CH2:35])([O:28][CH2:29][CH:30]=[CH2:31])[O:24][CH2:25][CH:26]=[CH2:27]>O=O.O>[P:23]([O:28][CH2:29][CH:30]=[CH2:31])([O:32][CH2:33][CH:34]=[CH2:35])([O:24][CH2:25][CH:26]=[CH2:27])=[O:2]참가 물질
7
실험 절차
To 10 ml. of an aqueous solution containing 0.5 g. of sodium carbonate and 0.25 g. of sodium bicarbonate there is added a solution of 1.0 g. of potassium dichromate in 50 ml. of water, then 60 ml. of triallyl phosphite. The resulting mixture is stirred at 25°-30°C while passing in oxygen for eight hours. The aqueous layer is removed, leaving a 96% yield of substantially pure triallyl phosphate.
후처리
- additionof an aqueous solution containing 0.5 g
- customThe aqueous layer is removed
출처 및 근거
- ORD 기록
- ord-3d4fcfb61293495fb01615714ee984b2
- 출처 데이터셋
- uspto-grants-1976_02
- 특허 번호
- US03939229
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