Methyl iodide → HCID 20560022, 화합물

HRID 1579339노트

반응식

HRID 1579339 반응식
[I-:1].[NH+]1C=CC=C[CH:3]=1.[CH:8]([NH:10][C:11]1[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[CH:21][C:12]=1[CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=1)=[O:9].CI.C(NC1C=CC=CC=1CCC1C=CC=CN=1)=O>>[I-:1].[CH:8]([NH:10][C:11]1[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[CH:21][C:12]=1[CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N+:16]=1[CH3:3])=[O:9]

참가 물질

5

반응물 4

HCID 6328Methyl iodideHCID 20559958HCID 20559958, 화합물HCID 20559985HCID 20559985, 화합물HCID 21863515PyridiuM iodide

생성물 1

HCID 20560022HCID 20560022, 화합물수율 95%

실험 절차

The pyridinium iodide is obtained by treating 2-(2-formamido-5-methoxyphenethyl)pyridine with methyl iodide according to the procedure described in Example 2c for 2-(o-formamidophenethyl)pyridine. Analytically pure 2-(2-formamido-5-methoxyphenethyl)-1-methylpyridinium iodide is obtained in a yield of 95% and has a melting point of 184°-186.5°C. (corr.).

출처 및 근거

ORD 기록
ord-d975ef4fd150411dabc346333fbe9872
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03931195

반응 노트

불러오는 중…