Methyl iodide → HCID 20559968, 화합물

HRID 1579347노트

반응식

HRID 1579347 반응식
[CH2:1]([C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=2[NH:17][CH:18]=[O:19])=[N:7][CH:8]=1)[CH3:2].C[I:21].[CH:22](NC1C=CC=CC=1CCC1C=CC=CN=1)=O>CC(C)=O>[I-:21].[CH2:1]([C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=2[NH:17][CH:18]=[O:19])=[N+:7]([CH3:22])[CH:8]=1)[CH3:2]

참가 물질

5

반응물 3

HCID 6328Methyl iodideHCID 20559958HCID 20559958, 화합물HCID 20560054HCID 20560054, 화합물

생성물 1

HCID 20559968HCID 20559968, 화합물수율 74%

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

Reaction of 5-ethyl-2-(o-formamidophenethyl)pyridine with methyl iodide in acetone according to the procedure of Example 2c for 2-(o-formamidophenethyl)pyridine provides a 74% yield of analytically pure 5-ethyl-2-(o-formamidophenethyl)-1-methylpyridinium iodide having a melting point of 134.5°-136.5°C.

출처 및 근거

ORD 기록
ord-84f17432f69b4180b504a6f2bd879652
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03931195

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