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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1579922생성일: 2026년 10월 26일

Benzylamine → 1,3,5-Triazin-2-amine, N-(phenylmethyl)-4,6-bis(trichloromethyl)-

https://huagongshe.com/reaction/1579922

반응식

참여 물질

역할이름HCID투입량
반응물BenzylamineHCID 7504—
반응물TriethylamineHCID 8471—
반응물1,3,5-Triazine, 2,4,6-tris(trichloromethyl)-HCID 23038—
용매BenzeneHCID 241—
생성물1,3,5-Triazin-2-amine, N-(phenylmethyl)-4,6-bis(trichloromethyl)-HCID 3264484.7%

반응 단계

Benzylamine (3.21 g., 0.03 mole) is added to 2,4,6-tris(trichloromethyl)-s-triazine (13 g., 0.03 mole) in dry benzene (75 ml.). Triethylamine (3.24 g., 0.03 mole) is then added to the reaction mixture and the solution set aside for 3 days. Evaporation to a residual oil and crystallization from methanol-water (9:1) gives the product 10.7 g., 85%, m.p. 96.5°-97°.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US03932167
출처 데이터셋uspto-grants-1976_01
ORD IDord-9e765a23e0ad444884fe0b6caa84d26a
출처 메모uspto-grants-1976_01