Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → 1,3,5-Triazin-2-amine, N-(phenylmethyl)-4,6-bis(trichloromethyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 1,3,5-Triazine, 2,4,6-tris(trichloromethyl)- | HCID 23038 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 1,3,5-Triazin-2-amine, N-(phenylmethyl)-4,6-bis(trichloromethyl)- | HCID 32644 | 84.7% |
반응 단계
Benzylamine (3.21 g., 0.03 mole) is added to 2,4,6-tris(trichloromethyl)-s-triazine (13 g., 0.03 mole) in dry benzene (75 ml.). Triethylamine (3.24 g., 0.03 mole) is then added to the reaction mixture and the solution set aside for 3 days. Evaporation to a residual oil and crystallization from methanol-water (9:1) gives the product 10.7 g., 85%, m.p. 96.5°-97°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03932167 |
| 출처 데이터셋 | uspto-grants-1976_01 |
| ORD ID | ord-9e765a23e0ad444884fe0b6caa84d26a |
| 출처 메모 | uspto-grants-1976_01 |