反应详情

Benzylamine (3.21 g., 0.03 mole) is added to 2,4,6-tris(trichloromethyl)-s-triazine (13 g., 0.03 mole) in dry benzene (75 ml.). Triethylamine (3.24 g., 0.03 mole) is then added to the reaction mixture and the solution set aside for 3 days. Evaporation to a residual oil and crystallization from methanol-water (9:1) gives the product 10.7 g., 85%, m.p. 96.5°-97°.

1. customEvaporation
2. customto a residual oil and crystallization from methanol-water (9:1)