Bis(eta-cyclopentadienyl) iron → HCID 178500169, 화합물

HRID 1579926노트

반응식

HRID 1579926 반응식
[CH-:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH-:6]1[CH:10]=[CH:9][CH:8]=[CH:7]1.[Fe+2:11].[C:12]([O:19][CH3:20])(=[O:18])[CH2:13][CH2:14][C:15]([CH3:17])=O>CO.C1CCCCC1>[C-:1]1([C:15]([C-:6]2[CH:10]=[CH:9][CH:8]=[CH:7]2)([CH3:17])[CH2:14][CH2:13][C:12]([O:19][CH3:20])=[O:18])[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH-:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[Fe+2:11].[CH-:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[Fe+2:11]

참가 물질

4

반응물 2

HCID 7611Bis(eta-cyclopentadienyl) ironHCID 69354Methyl levulinate

생성물 1

HCID 178500169HCID 178500169, 화합물

시약·촉매·용매 1

HCID 22386193Methanol cyclohexane용매

실험 절차

REACTING FERROCENE AND METHYL LEVULINATE IN THE PRESENCE OF AN ACID SUCH AS POLYPHOSPHORIC ACID AND A METHANOL-CYCLOHEXANE SOLVENT AT A TEMPERATURE OF FROM 76° TO 78°C to produce methyl 4, 4-diferrocenylpentanoate; and

후처리

  1. customA TEMPERATURE OF FROM 76° TO 78°C

출처 및 근거

ORD 기록
ord-85727d981b594d8fb9534f32b1bbf41c
출처 데이터셋
uspto-grants-1976_01
특허 번호
US03932240

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