Diisobutylamine → Lithium diisobutylamide
반응식
C([Li:5])CCC.[CH2:6]([NH:10][CH2:11][CH:12]([CH3:14])[CH3:13])[CH:7]([CH3:9])[CH3:8]>CCCCCC>[CH2:6]([N-:10][CH2:11][CH:12]([CH3:14])[CH3:13])[CH:7]([CH3:9])[CH3:8].[Li+:5]참가 물질
4
반응 조건
- 온도
- 20 °C
실험 절차
4 ml n-butyl-lithium solution and 1.38 ml di-i-butylamine are added to 1 l n-hexane and the mixture is stirred for 15 minutes at 20°C with exclusion of air and moisture. A solution of lithium di-i-butylamide is obtained.
출처 및 근거
- ORD 기록
- ord-00acaa52d6ff4177b092aff365baddc3
- 출처 데이터셋
- uspto-grants-1976_01
- 특허 번호
- US03935177
반응 노트
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