p-Anisoyl chloride → HCID 21561634, 화합물
반응식
Cl.[OH:2][CH2:3][C:4]1[CH:5]=[C:6]([OH:11])[C:7]([CH3:10])=[N:8][CH:9]=1.[C:12](Cl)(=[O:21])[C:13]1[CH:18]=[CH:17][C:16]([O:19][CH3:20])=[CH:15][CH:14]=1>N1C=CC=CC=1>[OH:2][CH2:3][C:4]1[CH:5]=[C:6]([O:11][C:12](=[O:21])[C:13]2[CH:18]=[CH:17][C:16]([O:19][CH3:20])=[CH:15][CH:14]=2)[C:7]([CH3:10])=[N:8][CH:9]=1참가 물질
4
실험 절차
To a solution of 0.9 g. of 5-hydroxymethyl-2-methyl-3-pyridinol hydrochloride in 5 ml. of anhydrous pyridine was added 0.86 g. of p-anisoyl chloride dropwise under cooling. After standing overnight the resulting mixture was poured into ice water and extracted with chloroform.
후처리
- extractionextracted with chloroform
출처 및 근거
- ORD 기록
- ord-15bcc5cc87684b72b11f6ed65c6b3fbf
- 출처 데이터셋
- uspto-grants-1976_01
- 특허 번호
- US03935311
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