Nitric Acid → 1,5-Diaminonaphthalene

HRID 1582791

반응식

[N+]([O-])(O)=O.[N+:5]([C:8]1[C:17]2[C:12](=[C:13]([N+:18]([O-])=O)[CH:14]=[CH:15][CH:16]=2)[CH:11]=[CH:10][CH:9]=1)([O-])=O>>[NH2:5][C:8]1[C:17]2[C:12](=[C:13]([NH2:18])[CH:14]=[CH:15][CH:16]=2)[CH:11]=[CH:10][CH:9]=1

참가 물질

반응물 2

HCID 944Nitric Acid

HCID 118031,5-Dinitronaphthalene

생성물 1

HCID 167201,5-Diaminonaphthalene

실험 절차

The invention also provides a process for the production of 1,5-diisocyanatonaphthalene in which naphthalene and/or 1-nitronaphthalene is reacted with nitric acid in the presence of a zeolite, the resulting 1,5-dinitronaphthalene is then hydrogenated to form 1,5-diaminonaphthalene and the resulting 1,5-diaminonaphthalene is phosgenated to form 1,5-diisocyanatonaphthalene.

출처 및 근거

ORD 기록: ord-055ff33f3e774fe5a625c81cac472510
출처 데이터셋: uspto-grants-2004_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06737554B2

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