Hydrochloric Acid → HCID 13430196, 화합물

HRID 1583743노트

반응식

HRID 1583743 반응식
C(OC([NH:8][CH2:9][C:10]([NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[C:19]1[O:24][C:23](=[O:25])[C:22]2[CH:26]=[CH:27][CH:28]=[CH:29][C:21]=2[N:20]=1)=[O:11])=O)(C)(C)C.[ClH:30]>C(OCC)(=O)C>[ClH:30].[NH2:8][CH2:9][C:10]([NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[C:19]1[O:24][C:23](=[O:25])[C:22]2[CH:26]=[CH:27][CH:28]=[CH:29][C:21]=2[N:20]=1)=[O:11]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 20258244HCID 20258244, 화합물

생성물 1

HCID 13430196HCID 13430196, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

2-[2-(tert-butyloxycarbonyl)aminoethanoyl]aminophenyl-3,1-benzoxazin-4-one (45 mg) was reacted in ethyl acetate with hydrogen chloride under reaction conditions as described for the synthesis of compounds of Example 9, Method A, to afford the above-titled compound.

출처 및 근거

ORD 기록
ord-39ef339885d542b9adac530082649cd0
출처 데이터셋
uspto-grants-1985_11
특허 번호
US04554272

반응 노트

불러오는 중…