Allyl Mercaptan → HCID 9794329, 화합물

HRID 1585988노트

반응식

HRID 1585988 반응식
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH3:6][O:7][C:8]1[N:9]=[N:10][C:11](Cl)=[C:12]([CH3:15])[C:13]=1[CH3:14]>CO>[CH3:6][O:7][C:8]1[N:9]=[N:10][C:11]([S:5][CH2:2][CH:3]=[CH2:4])=[C:12]([CH3:15])[C:13]=1[CH3:14]

참가 물질

5

반응물 3

HCID 13367Allyl MercaptanHCID 5360545SodiumHCID 212176653-Chloro-6-methoxy-4,5-dimethylpyridazine

생성물 1

HCID 9794329HCID 9794329, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

0.23 g(0.01 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 0.93 ml(0.01 mol) of allylmercaptan. To this mixture was added 1.73 g(0.01 mol) of 3-methoxy-4,5-dimethyl-6-chloropyridazine obtained from Preparation 5. The reaction solution was refluxed for one hour and then treated according to the same manner as Example 1 to obtain the title compound as a freezing pale white crystal.

후처리

  1. customobtained from Preparation 5
  2. temperatureThe reaction solution was refluxed for one hour
  3. additiontreated

출처 및 근거

ORD 기록
ord-ecd857d5b5914f38a47db573be880587
출처 데이터셋
uspto-grants-1999_08
특허 번호
US05942511

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