Allyl Mercaptan → HCID 10198535, 화합물
반응식
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH3:6][O:7][C:8]1[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:11](Cl)=[N:10][N:9]=1>CO>[CH3:6][O:7][C:8]1[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[C:11]([S:5][CH2:2][CH:3]=[CH2:4])=[N:10][N:9]=1참가 물질
5
실험 절차
0.23 g(0.01 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 0.93 ml(0.01 mol) of allylmercaptan. To this mixture was added 1.95 g(0.01 mol) of 1-methoxy-4-chlorophthalazine obtained from Preparation 7. The reaction solution was refluxed for one hour and then treated according to the same manner as Example 1 to obtain the title compound as a freezing pale white crystal.
후처리
- customobtained from Preparation 7
- temperatureThe reaction solution was refluxed for one hour
- additiontreated
출처 및 근거
- ORD 기록
- ord-fed89c9846f7463d81bd519cb371368c
- 출처 데이터셋
- uspto-grants-1999_08
- 특허 번호
- US05942511
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