Allyl Mercaptan → HCID 21217666, 화합물

HRID 1585991노트

반응식

HRID 1585991 반응식
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:8][C:9]1[N:10]=[N:11][C:12](Cl)=[CH:13][CH:14]=1)[CH3:7]>CO>[CH2:6]([O:8][C:9]1[N:10]=[N:11][CH:12]=[CH:13][C:14]=1[S:5][CH2:2][CH:3]=[CH2:4])[CH3:7]

참가 물질

5

반응물 3

HCID 13367Allyl MercaptanHCID 2615793-Chloro-6-ethoxypyridazineHCID 5360545Sodium

생성물 1

HCID 21217666HCID 21217666, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

0.57 g(0.025 mol) of metallic sodium was dissolved in 40 ml of absolute methanol and then mixed with 2.49 ml(0.025 mol) of allylmercaptan. To this mixture was added 3.96 g(0.025 mol) of 3-ethoxy-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a freezing pale white crystal.

후처리

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

출처 및 근거

ORD 기록
ord-b78a413db91a4584925d9e7c9d806fe9
출처 데이터셋
uspto-grants-1999_08
특허 번호
US05942511

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