Allyl Mercaptan → Pyridazine, 3-(2-propenylthio)-6-propoxy-
반응식
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:9][C:10]1[N:11]=[N:12][C:13](Cl)=[CH:14][CH:15]=1)[CH2:7][CH3:8]>CO>[CH2:6]([O:9][C:10]1[N:11]=[N:12][C:13]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:14][CH:15]=1)[CH2:7][CH3:8]참가 물질
5
실험 절차
1.15 g(0.05 mol) of metallic sodium was dissolved in 75 ml of absolute methanol and then mixed with 4.98 ml(0.05 mol) of allylmercaptan. To this mixture was added 8.63 g(0.05 mol) of 3-(n-propoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oily residue.
후처리
- temperatureThe reaction solution was refluxed for 24 hours
- additiontreated
출처 및 근거
- ORD 기록
- ord-0a471fdb725042d98a5fc22967d9fb5c
- 출처 데이터셋
- uspto-grants-1999_08
- 특허 번호
- US05942511
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