Allyl Mercaptan → HCID 10130734, 화합물

HRID 1585997노트

반응식

HRID 1585997 반응식
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:10][C:11]1[N:12]=[N:13][C:14](Cl)=[CH:15][CH:16]=1)[CH2:7][CH2:8][CH3:9]>CO>[CH2:6]([O:10][C:11]1[N:12]=[N:13][C:14]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:15][CH:16]=1)[CH2:7][CH2:8][CH3:9]

참가 물질

5

반응물 3

HCID 13367Allyl MercaptanHCID 2528253-butoxy-6-chloropyridazineHCID 5360545Sodium

생성물 1

HCID 10130734HCID 10130734, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

1.15 g(0.05 mol) of metallic sodium was dissolved in 75 ml of absolute methanol and then mixed with 4.98 ml(0.05 mol) of allylmercaptan. To this mixture was added 9.33 g(0.05 mol) of 3-(n-butoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

후처리

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

출처 및 근거

ORD 기록
ord-c653d76dda1245b391a28e607699980c
출처 데이터셋
uspto-grants-1999_08
특허 번호
US05942511

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