Allyl Mercaptan → HCID 21217662, 화합물

HRID 1585999노트

반응식

HRID 1585999 반응식
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[C:6]([O:10][C:11]1[N:12]=[N:13][C:14](Cl)=[CH:15][CH:16]=1)([CH3:9])([CH3:8])[CH3:7]>CO>[C:6]([O:10][C:11]1[N:12]=[N:13][C:14]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:15][CH:16]=1)([CH3:9])([CH3:8])[CH3:7]

참가 물질

5

반응물 3

HCID 13367Allyl MercaptanHCID 27639573-(Tert-Butoxy)-6-ChloropyridazineHCID 5360545Sodium

생성물 1

HCID 21217662HCID 21217662, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

0.46 g(0.02 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 1.99 ml(0.02 mol) of allylmercaptan. To this mixture was added 3.75 g(0.02 mol) of 3-(t-butoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

후처리

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

출처 및 근거

ORD 기록
ord-9c6696d76fa54e988979e37f461f3190
출처 데이터셋
uspto-grants-1999_08
특허 번호
US05942511

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