Allyl Mercaptan → HCID 10219981, 화합물

HRID 1586002노트

반응식

HRID 1586002 반응식
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[OH:6][CH2:7][CH2:8][O:9][C:10]1[N:11]=[N:12][C:13](Cl)=[CH:14][CH:15]=1>CO>[OH:6][CH2:7][CH2:8][O:9][C:10]1[N:11]=[N:12][C:13]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:14][CH:15]=1

참가 물질

5

반응물 3

HCID 13367Allyl MercaptanHCID 5360545SodiumHCID 14343567122913-80-8

생성물 1

HCID 10219981HCID 10219981, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

0.23 g(0.01 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 1.00 ml(0.01 mol) of allylmercaptan. To this mixture was added 1.75 g(0.01 mol) of 3-(2-hydroxyethoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale white needle crystal.

후처리

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

출처 및 근거

ORD 기록
ord-fd34e192f5ca401d8e966cabc950c911
출처 데이터셋
uspto-grants-1999_08
특허 번호
US05942511

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