Hexanoic acid, 2-bromo-, methyl ester → HCID 13706743, 화합물
반응식
Br[CH:2]([CH2:7][CH2:8][CH2:9][CH3:10])[C:3]([O:5][CH3:6])=[O:4].[F-:11].[K+]>C(N)(=O)C>[F:11][CH:2]([CH2:7][CH2:8][CH2:9][CH3:10])[C:3]([O:5][CH3:6])=[O:4]참가 물질
4
반응 조건
- 온도
- 105 °C
실험 절차
Methyl 2-bromocaproate (40 g) was added to anhydrous potassium fluoride (23 g) in acetamide (23 g) kept at 105° C. The mixture was vigorously stirred at 105° C. for 6 hours. The crude product obtained after the conventional work-up was distilled. Yield; 20 g (71 %), b.p.; 66° C./20 mmHg
후처리
- customkept at 105° C
출처 및 근거
- ORD 기록
- ord-29a8566348004da5a9a02deef3027dfa
- 출처 데이터셋
- uspto-grants-1993_06
- 특허 번호
- US05221763
반응 노트
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