Glycine → Glyphosate

반응식

[CH:1]([P:3](=[O:6])([OH:5])[OH:4])=O.[NH2:7][CH2:8][C:9]([OH:11])=[O:10]>>[CH2:8]([NH:7][CH2:1][P:3]([OH:4])([OH:5])=[O:6])[C:9]([OH:11])=[O:10]

참가 물질

반응물 2

HCID 750Glycine

HCID 10154022Formylphosphonic Acid

생성물 1

HCID 3496Glyphosate수율 90%

실험 절차

Reaction of formylphosphonic acid and glycine was carried out under the conditions described in Example 6 except that the pH was adjusted to 10.0 before commencement of the reduction reaction. Analysis indicated a 90.0% yield of glyphosate salts.

후처리

customwas adjusted to 10.0 before commencement of the reduction reaction

출처 및 근거

ORD 기록: ord-cef81218ec8b444099534f6233389600
출처 데이터셋: uspto-grants-1986_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04568432

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