Hydrochloric Acid → 1-(Chloromethoxy)hexane

HRID 1589235노트

반응식

HRID 1589235 반응식
[CH2:1]=[O:2].[CH2:3](O)[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[ClH:10]>ClC(Cl)CCl>[Cl:10][CH2:1][O:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 712FormaldehydeHCID 81031-Hexanol

생성물 1

HCID 125465121-(Chloromethoxy)hexane

시약·촉매·용매 1

HCID 65741,1,2-Trichloroethane용매

실험 절차

30 g (1 mole) of paraformaldehyde were stirred in 100 ml of 1,1,2-trichloroethane with 102 g (1 mole) of 1-hexanol at 0°-5° C. HCl gas was passed for 2 hours. The product is diluted to give a stock solution of 3M concentration.

후처리

  1. additionThe product is diluted
  2. customto give
  3. concentrationa stock solution of 3M concentration

출처 및 근거

ORD 기록
ord-e79d6e2b0572444ead572316f50326f0
출처 데이터셋
uspto-grants-1986_02
특허 번호
US04568700

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