Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Glycine → O-Benzyl-N-(tert-butoxycarbonyl)-L-serylglycine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Glycine | HCID 750 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | Boc-Ser(Bzl)-OSu | HCID 12879025 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | O-Benzyl-N-(tert-butoxycarbonyl)-L-serylglycine | HCID 14608022 | — |
반응 단계
To an aqueous solution containing 6.80 g of H-Gly-OH and 9.20 g of sodium hydrogen carbonate, under ice-cooling condition, was added 120 ml of THF solution containing 27.5 g of Boc-Ser(Bzl)-OSu, and the mixture was stirred at room temperature overnight.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05204326 |
| 출처 데이터셋 | uspto-grants-1993_04 |
| ORD ID | ord-f981639275ce4afcb212119f5339d2a8 |
| 출처 메모 | uspto-grants-1993_04 |