Thiourea → HCID 21699321, 화합물
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[NH2:1][C:2]([NH2:4])=[S:3].[Cl:5][C:6]1[C:7](=[O:15])[NH:8][C:9](=[O:14])[NH:10][C:11]=1[CH2:12]Cl>C(O)C>[ClH:5].[Cl:5][C:6]1[C:7](=[O:15])[NH:8][C:9](=[O:14])[NH:10][C:11]=1[CH2:12][S:3][C:2](=[NH:4])[NH2:1]참가 물질
4
실험 절차
To a solution of 140 mg of thiourea in ethanol (3 ml), 300 mg of 5-chloro-6-chloromethyluracil were added, followed by heating for 6 hours under reflux. After the reaction mixture was allowed to cool down, a crystallized matter was collected by filtration, whereby 337 mg of the title compound were obtained (yield: 81%).
후처리
- temperatureby heating for 6 hours
- temperatureunder reflux
- temperatureto cool down
- filtrationa crystallized matter was collected by filtration
출처 및 근거
- ORD 기록
- ord-d3f45cc67551406aad5bf00705952762
- 출처 데이터셋
- uspto-grants-2001_09
- 특허 번호
- US06294535B1
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