3-Chloroaniline → Benzenamine, 3-chloro-, hydrochloride (1:1)

HRID 1602227

반응식

HRID 1602227 반응식
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][CH:8]=1)[NH2:5]>Cl.CO>[ClH:1].[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][CH:8]=1)[NH2:5]

참가 물질

4

반응물 1

HCID 79323-Chloroaniline

생성물 1

HCID 67336Benzenamine, 3-chloro-, hydrochloride (1:1)

시약·촉매·용매 2

HCID 313Hydrochloric Acid용매HCID 887Methanol용매

실험 절차

60 g (0.47 mol) of 3-chloro-aniline are dissolved in 255 ml (0.56 mol) of a 2.2N solution of HCl in methanol. Concentration and stirring of the residue in diethyl ether, followed by filtering and drying, yield 3-chloro-aniline hydrochloride.

후처리

  1. concentrationConcentration
  2. filtrationby filtering
  3. customdrying

출처 및 근거

ORD 기록
ord-716cca8cf89f4b078fd6676e238ea6d7
출처 데이터셋
uspto-grants-1999_11
특허 번호
US05981533

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