Hydrochloric Acid → HCID 22008800, 화합물

HRID 1602615노트

반응식

HRID 1602615 반응식
[O:1]=[C:2]1[CH:7]([CH2:8][CH2:9][C:10]2[CH:19]=[CH:18][C:17]3[CH2:16][CH2:15][CH2:14][NH:13][C:12]=3[N:11]=2)[CH2:6][CH2:5][CH2:4][N:3]1[CH2:20][C:21]([O:23]CC)=[O:22].Cl>>[O:1]=[C:2]1[CH:7]([CH2:8][CH2:9][C:10]2[CH:19]=[CH:18][C:17]3[CH2:16][CH2:15][CH2:14][NH:13][C:12]=3[N:11]=2)[CH2:6][CH2:5][CH2:4][N:3]1[CH2:20][C:21]([OH:23])=[O:22]

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 22008742HCID 22008742, 화합물

생성물 1

HCID 22008800HCID 22008800, 화합물

실험 절차

A solution of 1-7 (71 mg, 0.21 mmol) and 6N HCl (15 mL) was stirred at 55° C. for 2 h, followed by concentration to give 1-8 as a pale yellow gum. TLC Rf =0.09 (silica, 20% CH3OH/EtOAc)

후처리

  1. concentrationfollowed by concentration

출처 및 근거

ORD 기록
ord-c2d20ed130414fc998b2e04e1ff4cd37
출처 데이터셋
uspto-grants-1999_11
특허 번호
US05981546

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