2'-Bromoacetophenone → HCID 23449301, 화합물

HRID 1603494

반응식

HRID 1603494 반응식
C(O[C:6]([NH:8][CH2:9][C:10](=[S:12])[NH2:11])=O)(C)(C)C.Br[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[C:20](=O)[CH3:21]>>[C:15]1([C:20]2[N:11]3[CH:6]=[N:8][CH:9]=[C:10]3[S:12][CH:21]=2)[CH:16]=[CH:17][CH:18]=[CH:19][CH:14]=1

참가 물질

3

반응물 2

HCID 750602'-BromoacetophenoneHCID 5324304tert-butyl N-(carbamothioylmethyl)carbamate

생성물 1

HCID 23449301HCID 23449301, 화합물수율 66%

실험 절차

The same procedure as in Preparation 10 was repeated except that 1.9 g of (N-t-butoxycarbonylamino) acetothioamide and 2.49 g of 2'-bromoacetophenone were used, thereby obtaining 1.32 g of the title compound.

후처리

  1. customThe same procedure as in Preparation 10

출처 및 근거

ORD 기록
ord-3f00dd7ac2f5416d86580babc3c1595f
출처 데이터셋
uspto-grants-1999_11
특허 번호
US05990101

연결된 노트

불러오는 중…