Hydrochloric Acid → 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide hydrochloride
반응식
[CH3:1][O:2][C:3]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=1)([CH2:8][N:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:10]1)[C:4]([NH:6][CH3:7])=[S:5].[ClH:21]>CCOCC>[ClH:21].[CH3:1][O:2][C:3]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=1)([CH2:8][N:9]1[CH2:10][CH2:11][O:12][CH2:13][CH2:14]1)[C:4]([NH:6][CH3:7])=[S:5]참가 물질
4
실험 절차
One gram of 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide in ether is added to ethereal hydrogen chloride. The resulting precipitate is filtered off and recrystallized from ethanol/ether to give 2-methoxy-N-methyl-3-morpholino-2-(2-pyridyl)thiopropanamide hydrochloride.
후처리
- filtrationThe resulting precipitate is filtered off
- customrecrystallized from ethanol/ether
출처 및 근거
- ORD 기록
- ord-83068ae0e12643a7893f4141c0ec8210
- 출처 데이터셋
- uspto-grants-1976_04
- 특허 번호
- US03948892
반응 노트
불러오는 중…