O-ethyl N-ethyl-N-cyclohexyl-thiocarbamate → Cycloate

HRID 1606417

반응식

HRID 1606417 반응식
[CH2:1]([N:3]([CH:9]1[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1)[C:4](=[S:8])[O:5]CC)[CH3:2].[CH2:15](N(CCC)C(=S)OCCC)[CH2:16]C>>[CH2:1]([N:3]([CH:9]1[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]1)[C:4](=[O:8])[S:5][CH2:15][CH3:16])[CH3:2]

참가 물질

3

반응물 2

HCID 21542996O-ethyl N-ethyl-N-cyclohexyl-thiocarbamateHCID 22226125Propyl di-n-propylthiocarbamate

생성물 1

HCID 14337Cycloate수율 80%

실험 절차

The procedure described in Example 4 is repeated but an equivalent amount of O-ethyl N-ethyl-N-cyclohexyl-thiocarbamate is substituted for O-propyl N,N-dipropyl-thiocarbamate. The title compound is obtaned with a yield of 80 %; b.p.: 142°-145°C/9 Hgmm., nD30 = 1.5049.

출처 및 근거

ORD 기록
ord-a7946ee5ba6c4aab9560df4da72b1906
출처 데이터셋
uspto-grants-1976_04
특허 번호
US03953427

연결된 노트

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