Dibenzothiophene → 2-Bromodibenzothiophene

HRID 1606768

반응식

HRID 1606768 반응식
[CH:1]1[C:9]2[C:8]3[CH:10]=[CH:11][CH:12]=[CH:13][C:7]=3[S:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[Br:14]Br>C(Cl)(Cl)Cl>[Br:14][C:2]1[CH:3]=[CH:4][C:5]2[S:6][C:7]3[CH:13]=[CH:12][CH:11]=[CH:10][C:8]=3[C:9]=2[CH:1]=1

참가 물질

4

반응물 2

HCID 3023DibenzothiopheneHCID 24408Bromine

생성물 1

HCID 2995082-Bromodibenzothiophene

시약·촉매·용매 1

HCID 6212Chloroform용매2회

실험 절차

Dibenzothiophene (27.6 g, 0.15 mole) was dissolved in 125 ml chloroform. Bromine (24.0 g, 0.15 mole) in 25 ml chloroform was added dropwise and the mixture was kept at room temperature for 23 hours.

출처 및 근거

ORD 기록
ord-01b88ce4d67f463ba4b974898f01360f
출처 데이터셋
uspto-grants-1976_04
특허 번호
US03953601

연결된 노트

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