참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | Acrylic Acid | HCID 6581 | — |
| 반응물 | Methyl Acrylate | HCID 7294 | — |
| 반응물 | Propylene glycol methyl ether acetate | HCID 7946 | — |
| 용매 | Methyl Isobutyl Ketone | HCID 7909 | — |
| 생성물 | Acrylic acid methyl acrylate | HCID 168350 | 54% |
반응 단계
9 g of acrylic acid, 1 g of methyl acrylate, 50 g of isobutyl methyl ketone, 50 g of propylene glycol methyl ether acetate and 3.0 g of AIBN were combined and heated to about 67° C. for 3 hours under an inert atmosphere (e.g., nitrogen gas). The precipitated polymer was washed with ethyl ether and vacuum dried to obtain pure poly(acrylic acid/methyl acrylate) resin (weight average molecular weight: 7200, yield: 54%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06984482B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_01 |
|---|
| ORD ID | ord-a2d1d2ff081c422e9147f0ad74d22d8a |
|---|
| 출처 메모 | uspto-grants-2006_01 |
|---|
