Benzoyl chloride → HCID 22258244, 화합물

HRID 1610836노트

반응식

HRID 1610836 반응식
[CH3:1][C:2]1[NH:6][C:5]2[CH2:7][CH2:8][CH2:9][CH:10]([CH3:11])[C:4]=2[N:3]=1.[C:12]([Cl:20])(=[O:19])[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C(#N)C>[ClH:20].[CH3:11][CH:10]1[C:4]2[N:3]=[C:2]([CH2:1][C:12]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)=[O:19])[NH:6][C:5]=2[CH2:7][CH2:8][CH2:9]1

참가 물질

4

반응물 2

HCID 7412Benzoyl chlorideHCID 22258232HCID 22258232, 화합물

생성물 1

HCID 22258244HCID 22258244, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

The compound is prepared as described in example XVII with 1.00 g (6.66 mmol) 2,4-Dimethyl-4,5,6,7-tetrahydro-1H-benzimidazole (example XI, step 1), 3.09 g (21.97 mmol) of benzoyl chloride and 2.36 g (23.30 mmol) of TEA in 20 ml acetonitrile.

후처리

  1. customThe compound is prepared

출처 및 근거

ORD 기록
ord-ac8aea67fe11455f8935b573deef973d
출처 데이터셋
uspto-grants-2006_01
특허 번호
US06984646B2

반응 노트

불러오는 중…