참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 1,4-Diazabicyclo(3.2.2)nonane | HCID 398407 | — |
| 반응물 | 4-Bromophenyl chloroformate | HCID 5237736 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Ssr-180711 | HCID 9797360 | — |
반응 단계
0.379 g (3.0 mmol) of 1,4-diazabicyclo[3.2.2]nonane and 0.84 ml (6.0 mmol) of triethylamine in 5 ml of dichloromethane are introduced into a 50-ml three-necked flask, the mixture is cooled to 0° C., 0.730 mg (3.1 mmol) of 4-bromophenyl chloroformate in solution in 3 ml of dichloromethane is added dropwise and the stirring is maintained at 0° C. for 10 min.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06987106B1 |
|---|
| 출처 데이터셋 | uspto-grants-2006_01 |
|---|
| ORD ID | ord-8d2c8fa26d724ab3b23780235a06e1f5 |
|---|
| 출처 메모 | uspto-grants-2006_01 |
|---|
