Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → Pyridinium, 1-(2-ethoxy-2-oxoethyl)-, bromide (1:1)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Ethyl bromoacetate | HCID 7748 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Pyridinium, 1-(2-ethoxy-2-oxoethyl)-, bromide (1:1) | HCID 87028 | — |
반응 단계
To a solution of 47.37 grams (0.599 mol) of pyridine in 300 milliters of acetonitrile over a period of approximately 5 minutes there was added 100.0 grams (0.599 mol) of ethyl bromoacetate. The mixture was then stirred for approximately 19.3 hours. Solid crystallized and was collected, washed with ether and dried. The yield of product was 113.3 grams (76.86% of theory); mp=133°-134° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05196538 |
| 출처 데이터셋 | uspto-grants-1993_03 |
| ORD ID | ord-f4391b37c25d4e478a60ba37f277cdb6 |
| 출처 메모 | uspto-grants-1993_03 |