Hydrochloric Acid → HCID 14822258, 화합물

HRID 1614562노트

반응식

HRID 1614562 반응식
[ClH:1].[NH2:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][C:12]([N:14]2[CH2:18][CH2:17][S:16][CH2:15]2)=[O:13])=[CH:5][CH:4]=1>>[ClH:1].[NH2:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][CH2:10][CH2:11][C:12]([N:14]2[CH2:18][CH2:17][S:16][CH2:15]2)=[O:13])=[CH:7][CH:8]=1

참가 물질

3

반응물 2

HCID 313Hydrochloric AcidHCID 14822257N-[4-(4-aminophenyl)butanoyl]thiazolidine

생성물 1

HCID 14822258HCID 14822258, 화합물수율 98%

실험 절차

To 5 ml of alcoholic hydrogen chloride 1 mmol of N-[4-(4-aminophenyl)butanoyl]thiazolidine was added and dissolved under heating. The mixture was stirred at room temperature for 2 hours. After the reaction, the solvent was evaporated under reduced pressure. To the residue was added anhydrous ether and precipitates thus produced were collected by filtration to obtain 0.28 g of colorless crystals of N-[4-(4-aminophenyl)butanoyl]thiazolidine hydrochloride (yield: 98%).

후처리

  1. dissolutiondissolved
  2. temperatureunder heating
  3. customAfter the reaction
  4. customthe solvent was evaporated under reduced pressure
  5. additionTo the residue was added anhydrous ether
  6. customprecipitates thus
  7. customproduced
  8. filtrationwere collected by filtration

출처 및 근거

ORD 기록
ord-dd4eea7a48f64c49a0fdc4e86b926e08
출처 데이터셋
uspto-grants-1993_03
특허 번호
US05198450

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