Nicotinic Acid → nicotinic acid, potassium salt

HRID 1627235노트

반응식

HRID 1627235 반응식
[OH-].[K+:2].[C:3]([OH:11])(=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[N:6][CH:5]=1>O>[C:3]([O-:11])(=[O:10])[C:4]1[CH:9]=[CH:8][CH:7]=[N:6][CH:5]=1.[K+:2]

참가 물질

4

반응물 2

HCID 938Nicotinic AcidHCID 14797Potassium Hydroxide

생성물 1

HCID 23668574nicotinic acid, potassium salt

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
50 °C

실험 절차

To a solution of KOH (1.12 g) in 10 ml of demineralised water, Nicotinic acid was added and stirred well at 50° C. for 3 h. Water was removed in a rotavapour. The solid was dried under vacuum at 120° C. to remove final traces of water to give 3.1 g of white solid with m.pt >325° C.

후처리

  1. customWater was removed in a rotavapour
  2. customThe solid was dried under vacuum at 120° C.
  3. customto remove final traces of water

출처 및 근거

ORD 기록
ord-3ae00697a9454965aab53fe4794ef412
출처 데이터셋
uspto-grants-2014_07
특허 번호
US08785529B2

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