1,4-Dibromobutane → HCID 18679514, 화합물

HRID 1633658노트

반응식

HRID 1633658 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:16]3[C:11](=[CH:12][C:13]([OH:17])=[CH:14][CH:15]=3)[CH:10]=[CH:9]2)=[CH:4][CH:3]=1.[Br:18][CH2:19][CH2:20][CH2:21][CH2:22]Br>>[Br:18][CH2:19][CH2:20][CH2:21][CH2:22][O:17][C:13]1[CH:12]=[C:11]2[C:16](=[CH:15][CH:14]=1)[N:8]([C:5]1[CH:6]=[CH:7][C:2]([Br:1])=[CH:3][CH:4]=1)[CH:9]=[CH:10]2

참가 물질

3

반응물 2

HCID 80561,4-DibromobutaneHCID 18679504HCID 18679504, 화합물

생성물 1

HCID 18679514HCID 18679514, 화합물

실험 절차

In analogy to example 3.1, 1-(4-Bromo-phenyl)-1H-indol-5-ol and 1,4-dibrombutane were converted to yield 5-(4-Bromo-butoxy)-1-(4-bromo-phenyl)-1H-indole as light yellow solid, mp 80-81° C., MS: 421 (M, 2Br).

출처 및 근거

ORD 기록
ord-13d72aecbade4d4884a6dc32df52346d
출처 데이터셋
uspto-grants-2003_01
특허 번호
US06503907B2

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