Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N-di-n-Butyl-2-benzyloxyacetamide → N,N-Dibutyl-2-hydroxyacetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N-di-n-Butyl-2-benzyloxyacetamide | HCID 18675619 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N,N-Dibutyl-2-hydroxyacetamide | HCID 11008655 | 111.1% |
반응 단계
4 g of N,N-di-n-butyl-2-benzyloxyacetamide were dissolved in 50 ml of ethanol, and a spatula tip of Pd/carbon was added. The mixture was stirred under a hydrogen atmosphere for 16 hours, and then the catalyst was filtered off and the solvent was distilled off. 3 g of an oil were isolated and were immediately reacted further.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06509341B1 |
| 출처 데이터셋 | uspto-grants-2003_01 |
| ORD ID | ord-a9fb9dcbd46a4b5199a190bd6340d452 |
| 출처 메모 | uspto-grants-2003_01 |