2-Tridecyn-1-ol → 1-Bromo-2-tridecyne

HRID 1635774

반응식

HRID 1635774 반응식
[CH2:1](O)[C:2]#[C:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13].C(Br)(Br)(Br)[Br:16].C1(P(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1>ClCCl>[Br:16][CH2:1][C:2]#[C:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

참가 물질

4

반응물 2

HCID 111169792-Tridecyn-1-olHCID 11387777CBr4 triphenylphosphine

생성물 1

HCID 186733851-Bromo-2-tridecyne

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

1-Bromo-2-tridecyne (colorless oil) was prepared from 2-tridecyn-1-ol using the CBr4/triphenylphosphine mixture in dichloromethane to carry out the halogenation. 1-Bromo-2-tridecyne (colorless oil) was thus formed with a yield of 91%.

출처 및 근거

ORD 기록
ord-ed1dc395dd2147808413d595d6032b70
출처 데이터셋
uspto-grants-2003_01
특허 번호
US06511670B1

연결된 노트

불러오는 중…