Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Tridecyn-1-ol → 1-Bromo-2-tridecyne
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Tridecyn-1-ol | HCID 11116979 | — |
| 반응물 | CBr4 triphenylphosphine | HCID 11387777 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 1-Bromo-2-tridecyne | HCID 18673385 | — |
반응 단계
1-Bromo-2-tridecyne (colorless oil) was prepared from 2-tridecyn-1-ol using the CBr4/triphenylphosphine mixture in dichloromethane to carry out the halogenation. 1-Bromo-2-tridecyne (colorless oil) was thus formed with a yield of 91%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06511670B1 |
| 출처 데이터셋 | uspto-grants-2003_01 |
| ORD ID | ord-ed1dc395dd2147808413d595d6032b70 |
| 출처 메모 | uspto-grants-2003_01 |