Benzyl Chloride → Dibenzyl sulfide
반응식
O.O.O.O.O.O.O.O.O.[S-2:10].[Na+].[Na+].[CH2:13](Cl)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>O>[CH2:13]([S:10][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1참가 물질
4
실험 절차
Sodium sulphide nonahydrate (2.40 g, 0.01 mol), benzyl chloride (1.26 g, 0.01 mol), water (3 ml) and compound 1 (0.5 mmol) were stirred at 70°-78° C. for 20 minutes. The reaction mixture was poured into water and left overnight at room temperature. The white crystals thus obtained were filtered off and dried to give 2.02 g of benzyl sulphide.
후처리
- customThe white crystals thus obtained
- filtrationwere filtered off
- customdried
출처 및 근거
- ORD 기록
- ord-1d2a958485814bccb29f50f62fb0ee9c
- 출처 데이터셋
- uspto-grants-1989_11
- 특허 번호
- US04880894
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