Sodium Hydroxide → HCID 15096390, 화합물

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[OH:1][CH2:2][C:3]([NH:5][CH:6]([C:12]([O:14]CC)=[O:13])[C:7]([O:9]CC)=[O:8])=[O:4].[OH-].[Na+:18]>>[OH:1][CH2:2][C:3]([NH:5][CH:6]([C:12]([O-:14])=[O:13])[C:7]([O-:9])=[O:8])=[O:4].[Na+:18].[Na+:18]

참가 물질

반응물 2

HCID 14798Sodium Hydroxide

HCID 150963891,3-Diethyl 2-[(2-hydroxyacetyl)amino]propanedioate

생성물 1

HCID 15096390HCID 15096390, 화합물

실험 절차

Diethyl 2-[(hydroxyacetyl)amino]malonate (0.56 g) is dissolved in 1N aqueous sodium hydroxide (5 ml), and the mixture is reacted at room temperature for 10 hours, and thereafter, the reaction mixture is concentrated under reduced pressure. The residue is washed with methanol to give disodium 2-[(hydroxyacetyl)amino]malonate (0.51 g).

후처리

customthe mixture is reacted at room temperature for 10 hours
concentrationthe reaction mixture is concentrated under reduced pressure
washThe residue is washed with methanol

출처 및 근거

ORD 기록: ord-5ecdab6a188f4da69a6a1e8d3cec2ada
출처 데이터셋: uspto-grants-1989_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04882447

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