Potassium Carbonate → Phenyl 6-methoxypyridin-3-ylcarbamate

HRID 1641979

반응식

HRID 1641979 반응식
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]([O:8][CH3:9])=[N:6][CH:7]=1.C(=O)([O-])[O-].[K+].[K+].Cl[C:17]([O:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)=[O:18]>CN1CCCC1=O>[C:20]1([O:19][C:17](=[O:18])[NH:1][C:2]2[CH:7]=[N:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=2)[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 15891Phenyl chloroformateHCID 811216-Methoxy-3-pyridinylamine

생성물 1

HCID 20185962Phenyl 6-methoxypyridin-3-ylcarbamate

시약·촉매·용매 1

HCID 13387N-methyl-2-pyrrolidone용매

실험 절차

5-amino-2-methoxy-pyridine (30 mg, 0.24 mmol) and potassium carbonate (167 mg, 1.20 mmol) are dissolved in N-methyl 2-pyrrolidone (1 ml). Phenyl chloroformate (36 μl, 0.29 mmol) is added and the reaction mixture is stirred at room temperature for 2 hours.

출처 및 근거

ORD 기록
ord-42d223cffd164cefbcf61fcc22d3a9e6
출처 데이터셋
uspto-grants-2012_02
특허 번호
US08114877B2

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