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Sodium Hydroxide → 3-[4-[(1,1-Dimethylethoxy)carbonyl]phenyl]propanoic acid benzyl ester

HRID 1647059
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인쇄 미리보기

반응식

HRID 1647059 반응식
S([O-])([O-])(=O)=O.C([N+](CCCC)(CCCC)CCCC)CCC.C([N+](CCCC)(CCCC)CCCC)CCC.[OH-].[Na+].[CH2:42]([O:49][C:50](=[O:66])[CH2:51]N=C(C1C=CC=CC=1)C1C=CC=CC=1)[C:43]1[CH:48]=[CH:47][CH:46]=[CH:45][CH:44]=1.Br[CH2:68][C:69]1[CH:81]=[CH:80][C:72]([C:73]([O:75][C:76]([CH3:79])([CH3:78])[CH3:77])=[O:74])=[CH:71][CH:70]=1>ClCCl.CCOCC>[CH2:42]([O:49][C:50](=[O:66])[CH2:51][CH2:68][C:69]1[CH:70]=[CH:71][C:72]([C:73]([O:75][C:76]([CH3:79])([CH3:78])[CH3:77])=[O:74])=[CH:80][CH:81]=1)[C:43]1[CH:44]=[CH:45][CH:46]=[CH:47][CH:48]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

7

반응물 4

HCID 14798Sodium HydroxideHCID 11414578Tert-butyl 4-(bromomethyl)benzoateHCID 11433187Bis(tetrabutylammonium) sulphateHCID 11782449Diphenylmethylene-Glycine benzyl ester

생성물 1

HCID 867465253-[4-[(1,1-Dimethylethoxy)carbonyl]phenyl]propanoic acid benzyl ester수율 36%

시약·촉매·용매 2

HCID 3283
Diethyl Ether
용매
HCID 6344Dichloromethane용매

실험 절차

Tetrabutyl ammonium sulfate (3.0 g, 9 mmol) was added to a biphasic mixture consisting of 10% aqueous sodium hydroxide (75 mL), 2-[(diphenylmethylene)amino]acetic acid benzyl ester (3.05 g, 9.3 mmol) and 1,1-dimethylethyl 4-bromomethylbenzoate (3.0 g, 9 mmol) in dichloromethane (58 mL). After several hours of vigorous stirring at room temperature, the reaction mixture was diluted with ether (300 mL) and the layers were separated. The organic layer was washed with water (3×30 mL), dried (K2CO3) and filtered. Concentration provided an oil that was purified by HPLC on silica gel (the columns were pre-treated with 10% triethylamine/hexanes, ethyl acetate and finally hexanes) eluting with a mixture of hexanes-ethyl acetate to give rac.-2-](diphenylmethylene)amino]-3-[4-[(1,1-dimethylethoxy)carbonyl]phenyl]propanoic acid benzyl ester, (1.7 g, 3 mmol) in 36% yield.

후처리

  1. customthe layers were separated
  2. washThe organic layer was washed with water (3×30 mL)
  3. dry with materialdried (K2CO3)
  4. filtrationfiltered
  5. concentrationConcentration
  6. customprovided an oil that
  7. customwas purified by HPLC on silica gel (the columns
  8. additionwere pre-treated with 10% triethylamine/hexanes, ethyl acetate and finally hexanes)
  9. washeluting with a mixture of hexanes-ethyl acetate

출처 및 근거

ORD 기록
ord-64e2a740e9364e50820298a4b8d45b2d
출처 데이터셋
uspto-grants-1993_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05182263

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