Sodium Carbonate → HCID 19921162, 화합물

HRID 1647890

반응식

HRID 1647890 반응식
[CH3:1][O:2][C:3]([CH2:5][CH2:6][NH:7][C:8]([C:10]1[CH:25]=[CH:24][C:13]2[N:14]([CH3:23])[C:15]([CH:17]3[CH2:22][CH2:21][NH:20][CH2:19][CH2:18]3)=[N:16][C:12]=2[CH:11]=1)=[O:9])=[O:4].Br.C(S[C:30](=[NH:32])[NH2:31])C.C(=O)([O-])[O-].[Na+].[Na+]>CN(C)C=O>[C:30]([N:20]1[CH2:21][CH2:22][CH:17]([C:15]2[N:14]([CH3:23])[C:13]3[CH:24]=[CH:25][C:10]([C:8]([NH:7][CH2:6][CH2:5][C:3]([O:2][CH3:1])=[O:4])=[O:9])=[CH:11][C:12]=3[N:16]=2)[CH2:18][CH2:19]1)(=[NH:31])[NH2:32]

참가 물질

5

반응물 3

HCID 10340Sodium CarbonateHCID 200213S-Ethylisothiuronium bromideHCID 19921265HCID 19921265, 화합물

생성물 1

HCID 19921162HCID 19921162, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

Prepared from 5-[(2-methoxycarbonyl-ethyl)-aminocarbonyl]-1-methyl-2-(4-piperidinyl)-benzimidazole and S-ethylisothiourea-hydrobromide by heating to 100° C. for 4 hours in dimethylformamide in the presence of sodium carbonate.

출처 및 근거

ORD 기록
ord-3203693e9a7b471988dc7a71f97095a1
출처 데이터셋
uspto-grants-1995_07
특허 번호
US05434150

연결된 노트

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